Alkali-fusion-based Removal of Vacuum-compatible Heat-resistant Epoxy Resins using KOH-NaOH Eutectic Melt

17 April 2025, Version 1
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

We propose a process for decomposing and removing vacuum-compatible heat-resistant epoxy resins adhered to vacuum components by alkali fusion. We demonstrated the reworking of Al2O3 substrates with printed electrode patterns from the worn-out qPlus sensors using KOH-NaOH eutectic melt under atmospheric pressure. The substrate was reworked with a high yield of 94 % for a heating temperature of 510 ℃ and a duration of 5 min. The proposed method is an efficient removal technique for vacuum-compatible heat-resistant epoxy resins that can be performed at the laboratory level without special reagents or equipment. It enables reworking a wide range of vacuum components sufficiently resistant to the alkali melt.

Keywords

Vacuum-compatible Epoxy Resin
Alkali Fusion
Thermal Degradation
qPlus AFM
Ultra-High Vacuum

Comments

Comments are not moderated before they are posted, but they can be removed by the site moderators if they are found to be in contravention of our Commenting Policy [opens in a new tab] - please read this policy before you post. Comments should be used for scholarly discussion of the content in question. You can find more information about how to use the commenting feature here [opens in a new tab] .
This site is protected by reCAPTCHA and the Google Privacy Policy [opens in a new tab] and Terms of Service [opens in a new tab] apply.