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Surfactant-assisted synthesis of titanium nanoMOFs for thin film fabrication

22 July 2021, Version 1
Working Paper
This content is a preprint and has not undergone peer review at the time of posting.

Abstract

We use dodecanoic acid as a modulator to yield titanium MOF nanoparticles with good control of size and colloid stability and minimum impact to the properties of the framework to enable direct fabrication of crystalline, porous thin films

Supplementary materials

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Supplementary information
Description
Experimental details; materials and reagents, synthesis of the NPs, PXRD, profile fitting, SEM, 1H-NMR, N2 isotherms, DLS, TEM, UV-Vis of the NPs and AFM and Kr isotherms of the film.
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Version History

Jul 22, 2021 Version 1

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The content is available under CC BY NC ND 4.0 [opens in a new tab]

DOI

10.26434/chemrxiv-2021-j48tn
D O I: 10.26434/chemrxiv-2021-j48tn [opens in a new tab]

Funding

European Research Council
ERC Stg Chem-fs-MOF 714122 and VAPORE 716472
Spanish Government
CEX2019-000919-M, RTI2018-098568-A-I00, CTQ2017-83486-P & RYC-2016-1981
Research Foundation Flanders
G083016N, G85720N and 12Z6520N

Author’s competing interest statement

The author(s) have declared they have no conflict of interest with regard to this content

Ethics

The author(s) declare that they have sought and gained approval from the relevant ethics committee/IRB for this research and its publication.

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